Key Lab Initiative

Center for Microwave Chemistry

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NETL’s microwave research holds the promise of disruptive innovation. It enables opportunities for substantial reductions in carbon emissions through reduced energy requirements, minimal direct emissions, and increased process selectivity.

The application of microwave fields to chemical processes may transform the way chemical reactions occur, with NETL focusing on ammonia synthesis, hydrogen generation, polymer and plastic conversion, and synthetic fuels conversion.

As we explore the unique properties of microwave-assisted catalysis (μWave) process intensification, we are investing in signature capabilities to accelerate the understanding of fundamental μWave phenomena.

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Why Partner With NETL?

NETL is looking for clients and partners to pursue this exciting field of applied energy research.

In addition to microwave catalysis leadership, we are developing a signature research infrastructure to conduct cutting-edge science studies of microwave reaction chemistry. This multi-year investment provides capabilities in experimental research pushing the boundaries of current scientific capabilities.

We look forward to shaping the future of energy with you!

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Facilities and Equipment

Microwave catalysis technology can open the next frontier of science in the chemical process industry, and NETL invested in the tools to pursue these opportunities.

  • ReACT Facility – state-of-the-art, 6,000 sq-ft+ Reaction Analysis and Chemical Transformation (ReACT) facility supports NETL’s energy conversion engineering competency and novel microwave approaches to selectively energize chemical reactions. No other known facility in the world has this capability.
  • Measurement at High Temperatures – Electromagnetic material characterization equipment includes one-of-a-kind test fixtures used for material characterization under a microwave field from room temperature to 1000°C.
  • Gas-Solid Microwave Reactor Systems – Pulsing single-mode microwave cavity from Sairem with fixed frequency (2.45 GHz) 2kW magnetron, a continuous variable frequency (2-8 GHz), 0.6kW microwave reactor from Lambda Technologies, Inc., and high-pressure (36 bar) microwave reactor (2.45 GHz, and 3 kW) from Malachite Technologies.
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Experience

NETL’s research includes fundamental, deep science and applied science benefits for accelerating new technologies. Our microwave team delivered high-impact early research and continues to provide “best in class” expertise to facilitate project goals.

In-situ surface reaction diagnostics aids our accomplishments, providing real time analysis of surface chemistry on a catalyst during a microwave-driven process. This fundamental characterization ability gives insight into the mechanism changes of a reaction under an electromagnetic field and assists in innovative catalyst development for microwave reactions.

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Our Unique Expertise

Breakthrough technology that increases selectivity toward desired products and economically viable applications. By utilizing microwave technology to develop a low temperature/pressure process, we created a flexible, modular scale version of the ammonia synthesis process. This includes rapid startup ammonia production with on-demand production of ammonia, enabling chemical storage of renewable energy or ammonia to fertilizer production.

Conducting research across the entire value chain for the hydrogen economy, from materials development to modular conversion processes to CCS and hydrogen uses in combustion/fuel cells. Our research has experimentally demonstrated viability of microwave technology by enhancing conversion, energy efficiency, and better integration with renewable energy sources.

NETL is assessing its commercial potential and scalability of the current research with multiple projects currently underway. One project focus is a rapid one-step process for catalytic deconstruction of plastic waste to hydrogen-rich syngas or specialized end products.

NETL is working to leverage biomass and other rich hydrocarbon sources for production of “value-added” fuel types. Through modular conversion processes and chemical reaction know how, our research is making syngas production easier, cheaper, and with less emission byproducts. Through selectivity enhancements with the catalyst, NETL is forging a transformational energy economy.

Contact

 

Dushyant Shekhawat
Supervisor, Reaction Engineering Team Energy Conversion Engineering Directorate
Dushyant.Shekhawat@netl.doe.gov

 
 
 

Randall Gemmen
Associate Director Energy Conversion Engineering Directorate
Randall.Gemmen@netl.doe.gov