This invention describes an improved method for extracting rare earth elements (REEs) from coal ash at ambient temperatures. This technology is available for licensing and/or further collaborative research from the U.S. Department of Energy’s National Energy Technology Laboratory.

Challenge
As China currently controls the supply and prices of almost all the world’s REEs, developing a domestic supply is critical for the continued manufacturing of technologies that support nearly all modern devices, including critical systems for energy and national defense. REE extraction efforts from domestic sources of coal and coal-related resources have emerged as a viable solution, but successful methods must be both cost-effective and environmentally friendly.

Current methods and technologies for REE extraction from ore and other sources can be hazardous and expensive to implement without harming the environment or workers. For example, common practices employ high temperatures and strong acids or bases. This technology seeks to overcome these and other issues with current REE extraction methods by turning to a material that is currently viewed as a waste – coal ash.

Research is active on the design and development of solid oxide fuel cell (SOFC) systems featuring thicker interconnects for increased thermal energy storage. A large amount of heat can then be extracted from the interconnects and used to quickly increase the electric load in a hybrid power system. This invention is available for licensing and/or further collaborative research from the U.S. Department of Energy’s National Energy Technology Laboratory (NETL).

The U.S. Department of Energy’s National Energy Technology Laboratory (NETL) has developed a laser induced breakdown spectroscopy (LIBS) probe featuring simplified construction that minimizes the need for optical elements from the probes data collection path, reducing potential interference with the transmission of high quality spectra. By reducing the complexity and cost of the laser head, the invention maximizes the amount and quality of light returned for analysis and increases the usefulness of LIBS research.

The Department of Energy’s National Energy Technology Laboratory (NETL) is seeking licensing partners interested in implementing United States Patent Number 7,421,166 titled "Laser Spark Distribution and Ignition System."

Disclosed in this patent is NETL’s laser spark distribution and ignition system, which reduces the high-power optical requirements normally needed for such a system by using optical fibers to deliver low-peak-energy pumping pulses to a laser amplifier or laser oscillator. Laser spark generators then produce a high-peak-power laser spark from a single low power pulse. The system has applications in natural gas fueled reciprocating engines, turbine combustors, explosives, and laser induced breakdown spectroscopy diagnostic sensors.

The invention is a new low-cost way to form an optical sensor array that monitors multiple parameters such as temperature and hydrogen in essential components of electrical transmission and distribution networks. It uses multi-wavelength interrogation combined with multiple sensor elements using a single optical fiber. This technology is available for licensing and/or further collaborative research from the U.S. Department of Energy’s National Energy Technology Laboratory.

Challenge

Power transformers are among the most essential components of electrical transmission and distribution networks. To avoid the substantial financial and social expenses caused by catastrophic failures, there is a growing need to develop low-cost and real-time analytical techniques and instruments to detect and diagnose fundamental changes in the operating characteristics of transformers. Key parameters, such as dissolved gases content and temperature, provide valuable information for assessing the condition of transformers. For example, dissolved gas analysis (DGA) identifies electrical or thermal faults in transformers. In addition, temperature information is vital because when the temperature in transformers exceeds 90o C, the aging rate of insulation and tensile strength grows, resulting in a dramatic deterioration of transformer life expectancy. It is therefore of significant value to monitor the temperature under various ambient and loading conditions to identify failures before they result in significant damages. 

This technology, titled "Metal Oxide Promoters for Improving the Reactivity and Capacity of Oxygen Carriers for the Chemical Looping Combustion Process,” provides a mixed metal oxide carrier to improve the oxygen transfer capacity and reactivity of existing carriers. Following patent approval, the technology will be available for licensing and/or further collaborative research from the U.S. Department of Energy’s National Energy Technology Laboratory.

This invention describes a system and method for rapid, ambient-temperature growth of metal-organic framework (MOF) films for gas sensor applications. More specifically, the invention relates to growth of MOF films on advanced sensor devices such as distributed optical fiber and passive wireless like surface acoustic wave-based sensors. This technology is available for licensing and/or further collaborative research from the U.S. Department of Energy’s National Energy Technology Laboratory.

Challenge

MOF thin films have emerged as particularly attractive candidates for gas sensing applications due to their tunable porosity and pore size, enabling them to be rationally designed to selectively absorb specific gasses of interest. MOFs are especially appealing due to their high selectivity and capacity for energy-relevant gasses such as carbon dioxide and methane. A critical step towards the development of MOF thin film devices is the ability to efficiently and reliably incorporate high-quality MOF layers onto a wide range of substrates like optical fibers. However, current techniques are often inconvenient due to long reaction times, heating requirements, equipment costs and/or poor control over crystal coverage and morphology.

Research is currently active on the patented technology "Method for Determining Solids Circulation Rate." The technology is available for licensing and/or further collaborative research from the U.S. Department of Energy’s National Energy Technology Laboratory.

Research is currently active on the following and patented technologies:

• "Regenerable Immobilized Aminosilane Sorbents for Carbon Dioxide Capture", known as the Basic Immobilized Amine Sorbent (BIAS) process
• "Regenerable Sorbent Technique for Capturing CO₂ Using Immobilized Amine Sorbents"

These technologies are available for licensing and/or further collaborative research from the U.S. Department of Energy’s National Energy Technology Laboratory.

The Department of Energy’s National Energy Technology Laboratory (NETL) is seeking licensing partners interested in implementing United States Patent Number 7,704,746 titled "Method of Detecting Leakage from Geologic Formations Used to Sequester CO₂."

Disclosed in this patent is a method to measure carbon dioxide leakage from sequestration reservoirs and, specifically, an enhanced method for the detection and quantification of carbon dioxide leaks from geologic formations. The method injects tracers along with the carbon dioxide, monitors leakage with gas chromatography, and provides early detection of leakage by measuring the leakage rates of other gases within the geologic formation.